N-[4-(Azetidin-1-ylsulfon­yl)phen­yl]-N-(2,4-difluoro­benz­yl)acetamide

نویسندگان

  • Jian-Mei Lin
  • Jia-Wen Li
  • Jing-Song Lv
چکیده

In the title mol-ecule, C(18)H(18)F(2)N(2)O(3)S, the dihedral angle between the benzene rings is 79.40 (11)°. The 2,4-difluoro-benzyl and azetidine fragments adopt a trans arrangement relative to the central benzene ring. In the crystal, weak C-H⋯O hydrogen bonds connect mol-ecules into a two-dimensional network parallel to (001).

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

2-Chloro-1-[4-(2,4-difluoro­benz­yl)piperazin-1-yl]ethanone

In the title mol-ecule, C(13)H(15)ClF(2)N(2)O, the piperazine ring is in a chair conformation with the 2,4-difluoro-benzyl and chloro-acetyl substituents in equatorial positions.

متن کامل

N-[4-(2-Propyn-1-yl­oxy)phen­yl]acetamide

The title compound, C(11)H(11)NO(2), was synthesized by chemoselective N-acetyl-ation of 4-amino-phenol followed by reaction with propargyl bromide in the presence of K(2)CO(3). the acetamide and propyn-1-yloxy substituents form dihedral angles of 18.31 (6) and 7.01 (10)°, respectively, with the benzene ring. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds into chains along [010]....

متن کامل

Facile synthesis and in vivo hypoglycemic activity of novel 2, 4- hiazolidinedione derivatives

A series of novel 2, 4-thiazolidinedione derivatives 2-{4-[(E)-(2,4-dioxo-1,3-thiazolidin-5-ylidene)methyl] phenoxy}N-(substituted phenyl) acetamides d (1-12) have been accomplished in good yields by stirring 2,4-thiazolidinedione a and 2-(4-formyl phenoxy) N-substituted acetamide c (1-12) at room temperature. Some of the reaction sequences were carried under microwave irradiation which resulte...

متن کامل

N-{4-[(E)-(4-Methyl­phen­yl)imino­meth­yl]phen­yl}acetamide

There are two symmetry-independent mol-ecules in the asymmetric unit of the title compound, C(16)H(16)N(2)O, that differ in conformation. The dihedral angles between the benzene rings in the two mol-ecules are 44.35 (19) and 48.14 (17)°, but the rings twist in opposite directions. The acetamide groups make nearly equal dihedral angles of 25.4 (3) and 25.7 (3)° with the parent benzene rings. An ...

متن کامل

N-[4-(4-Nitro­phen­oxy)phen­yl]acetamide

The asymmetric unit of the title compound, C(14)H(12)N(2)O(4), contains two mol-ecules that differ principally in the orientation of the acetamide substituent to the adjacent benzene ring with dihedral angles of 44.77 (7) and 19.06 (7)°. The dihedral angles between the benzene rings are 64.46 (4) and 80.84 (4)°. In the crystal, classical N-H⋯O hydrogen bonds form C(4) chains along [100]. These ...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

عنوان ژورنال:

دوره 68  شماره 

صفحات  -

تاریخ انتشار 2012